Use of Imaging Techniques to Quantify Fluid-Rock Interaction and Petrophysical Properties in Low Permeability Hydrocarbon Reservoirs

dc.contributor.advisorClarkson, Christopher R.
dc.contributor.authorDeglint, Hanford John
dc.contributor.committeememberSpencer, Ronald J.
dc.contributor.committeememberTutolo, Benjamin M.
dc.contributor.committeememberBryant, Steven L.
dc.contributor.committeememberMohanty, Kishore K.
dc.date2019-06
dc.date.accessioned2018-11-02T17:38:43Z
dc.date.available2018-11-02T17:38:43Z
dc.date.issued2018-11-01
dc.description.abstractLow permeability (‘tight’) reservoirs have become a viable source of hydrocarbons in North America because of horizontal drilling and multi-stage hydraulic fracturing. While commercial production continues for these unconventional resources, recovery of the available hydrocarbons (particularly liquids) remains low. This is due impart to the lack of understanding of the basic reservoir properties. Without advancing characterization methods for petrophysical and geomechanical properties, we can expect these inefficiencies in resource development to persist. This thesis begins to address this lapse in knowledge by using imaging techniques to quantify fluid-rock interaction and characterize petrophysical properties. In tight reservoirs, most of the hydrocarbon resource resides within the matrix nanopore structure. However, conventional characterization methods are not usually performed at this scale. Ultra-small-angle neutron scattering is employed to probe geological samples for determining the connected and unconnected porosity, including porosity at the nanoscale. This information can be used in tandem with 2D scanning electron microscope (SEM) images to populate pore network models which in turn are used to derive petrophysical properties. An important contribution of this thesis is the development of techniques to enable the imaging and quantification of wettability at the micro- and nanoscale. While imaging of rock nanopore pore structure is now routine, imaging of fluid-rock interaction at this scale, which is necessary for quantifying multi-phase fluid distribution and flow, is not. Using an environmental SEM, three approaches are employed: 1) condensation and evaporation, 2) cryogenic, and 3) micro-injection. Using a parametrized Young-Laplace model, contact angles (advancing/receding) and spontaneous imbibition rates are calculated. Fluid distributions in preserved core are determined. Macro- and micro-contact angles for the same sample are compared, revealing that contact angle variance in a small sample is large, even within sites a few millimetres apart. This suggests that macro-scale measurements do not appropriately capture the heterogeneity of low-permeability samples. Finally, using a combination of X-ray, SEM, and cathodoluminescence, a variety of rock petrophysical properties are determined from drill cuttings. Custom written software using advanced image processing techniques is used to automatically measure mineralogical composition, cementation, and porosity.en_US
dc.identifier.citationDeglint, H. J. (2018). Use of Imaging Techniques to Quantify Fluid-Rock Interaction and Petrophysical Properties in Low Permeability Hydrocarbon Reservoirs (Doctoral thesis, University of Calgary, Calgary, Canada). Retrieved from https://prism.ucalgary.ca. doi:10.11575/PRISM/33240en_US
dc.identifier.doihttp://dx.doi.org/10.11575/PRISM/33240
dc.identifier.urihttp://hdl.handle.net/1880/108944
dc.language.isoeng
dc.publisher.facultyGraduate Studies
dc.publisher.facultyScience
dc.publisher.institutionUniversity of Calgaryen
dc.publisher.placeCalgaryen
dc.rightsUniversity of Calgary graduate students retain copyright ownership and moral rights for their thesis. You may use this material in any way that is permitted by the Copyright Act or through licensing that has been assigned to the document. For uses that are not allowable under copyright legislation or licensing, you are required to seek permission.
dc.subject.classificationGeologyen_US
dc.subject.classificationMineralogyen_US
dc.subject.classificationEngineering--Petroleumen_US
dc.titleUse of Imaging Techniques to Quantify Fluid-Rock Interaction and Petrophysical Properties in Low Permeability Hydrocarbon Reservoirs
dc.typedoctoral thesis
thesis.degree.disciplineGeoscience
thesis.degree.grantorUniversity of Calgary
thesis.degree.nameDoctor of Philosophy (PhD)
ucalgary.item.requestcopytrue
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